2019 |
Gomez-Jeria, J S; Segura, C; Carcamo-Vega, J J Methodological problems in the analysis of the Raman spectra of the paper of some postage stamps from Crete Artículo de revista Chemistry Research Journal, 4 , pp. 58-67, 2019, ISSN: 2455-8990. Resumen | Enlaces | BibTeX | Etiquetas: baseline correction, cellulose, Cretan Postage stamps, Crete, fluorescence, raman spectroscopy, smooth., Vancouver Raman algorithm @article{RN1007, title = {Methodological problems in the analysis of the Raman spectra of the paper of some postage stamps from Crete}, author = {J.S. Gomez-Jeria and C. Segura and J.J. Carcamo-Vega}, url = {https://www.researchgate.net/publication/332547457_A_Raman_analysis_of_the_paper_of_some_postage_stamps_from_Crete}, issn = {2455-8990}, year = {2019}, date = {2019-01-06}, journal = {Chemistry Research Journal}, volume = {4}, pages = {58-67}, publisher = {Leon Publications}, abstract = {A Raman spectroscopy study has been carried out with 633 and 768 nm laser lines to characterize three Cretan postage stamps. The first corresponds was issued by the Russian Empire Administration area and the other two belong to the 1905 Revolutionary Issues. The resulting Raman spectra are not of enough quality allowing a direct interpretation. Possible corrections to these spectra are, for example, the removal of the background fluorescence, the baseline correction and/or smooth. These tools are available in several spectroscopy software packages. The central question is the reliability of the spectra obtained after one or more corrections are applied. In order to begin creating a common procedure to treat all samples we ascribed only those bands that coincide with the cellulose calculated Raman frequencies. The first results suggest that it is necessary to carry out more studies with a significant number of samples before proposing a common treatment for all Raman spectra of postage stamps presenting fluorescence.}, keywords = {baseline correction, cellulose, Cretan Postage stamps, Crete, fluorescence, raman spectroscopy, smooth., Vancouver Raman algorithm}, pubstate = {published}, tppubtype = {article} } A Raman spectroscopy study has been carried out with 633 and 768 nm laser lines to characterize three Cretan postage stamps. The first corresponds was issued by the Russian Empire Administration area and the other two belong to the 1905 Revolutionary Issues. The resulting Raman spectra are not of enough quality allowing a direct interpretation. Possible corrections to these spectra are, for example, the removal of the background fluorescence, the baseline correction and/or smooth. These tools are available in several spectroscopy software packages. The central question is the reliability of the spectra obtained after one or more corrections are applied. In order to begin creating a common procedure to treat all samples we ascribed only those bands that coincide with the cellulose calculated Raman frequencies. The first results suggest that it is necessary to carry out more studies with a significant number of samples before proposing a common treatment for all Raman spectra of postage stamps presenting fluorescence. |
Gomez-Jeria, J S; Gutierrez, S; Surco-Luque, J; Clavijo, E; Reyes-Diaz, I A Characterization Of Cellulose In Seven Books Using Raman Spectroscopy In The 800-1800 cm-1 Range. Artículo de revista Research Journal of Pharmaceutical, Biological and Chemical Sciences., 10 , pp. 1565-1579, 2019, ISSN: 2455-8990. Resumen | Enlaces | BibTeX | Etiquetas: alum, carbonate, cellulose, gelatin, lignin, Paper composition, raman spectroscopy, rosin, sulfate, Vancouver Raman algorithm. @article{RN1008, title = {A Characterization Of Cellulose In Seven Books Using Raman Spectroscopy In The 800-1800 cm-1 Range.}, author = {J.S. Gomez-Jeria and S. Gutierrez and J. Surco-Luque and E. Clavijo and I. Reyes-Diaz}, url = {https://www.researchgate.net/publication/330521781_A_characterization_of_cellulose_in_seven_books_using_Raman_spectroscopy_in_the_800-1800_cm-1_range}, issn = {2455-8990}, year = {2019}, date = {2019-01-03}, journal = {Research Journal of Pharmaceutical, Biological and Chemical Sciences.}, volume = {10}, pages = {1565-1579}, publisher = {2010 RJPBCS}, abstract = {Raman spectroscopy was employed to study the non-printed area of a page of seven books printed in the 18th and 19th centuries. We employed the Vancouver Raman Algorithm to deal with the strong fluorescence background, obtaining spectra only in the 800 a 1800 cm-1 range. Two samples contain lignin, suggesting the presence of wood fibers. One sample (year 1799) contains only cellulose and gelatin. Two samples contain rosin. There are several Raman bands that we could not ascribe. Based on the results we propose a way to prepare the samples that could guarantee that the infrared and Raman spectra can be compared with confidence.}, keywords = {alum, carbonate, cellulose, gelatin, lignin, Paper composition, raman spectroscopy, rosin, sulfate, Vancouver Raman algorithm.}, pubstate = {published}, tppubtype = {article} } Raman spectroscopy was employed to study the non-printed area of a page of seven books printed in the 18th and 19th centuries. We employed the Vancouver Raman Algorithm to deal with the strong fluorescence background, obtaining spectra only in the 800 a 1800 cm-1 range. Two samples contain lignin, suggesting the presence of wood fibers. One sample (year 1799) contains only cellulose and gelatin. Two samples contain rosin. There are several Raman bands that we could not ascribe. Based on the results we propose a way to prepare the samples that could guarantee that the infrared and Raman spectra can be compared with confidence. |
2014 |
Osorio, F; Diaz-Fleming, G; Martinez, U; Campos-Vallette, M; Clavijo, E; Aliaga, A E; Espinosa, M F; Bracchitta, D Micro-Raman Spectroscopy of Decorated Pottery of the Diaguita Culture from Iv Region, Chile (9th-15th Century Ad) Artículo de revista Journal of the Chilean Chemical Society, 59 (3), pp. 2619-2621, 2014, ISSN: 0717-9707. Resumen | Enlaces | BibTeX | Etiquetas: analysis, ancient, archaeology, archaeometry, art ceramics, diaguita identification, iron-oxides, pigment pigments, raman spectroscopy @article{RN209, title = {Micro-Raman Spectroscopy of Decorated Pottery of the Diaguita Culture from Iv Region, Chile (9th-15th Century Ad)}, author = { F. Osorio and G. Diaz-Fleming and U. Martinez and M. Campos-Vallette and E. Clavijo and A.E. Aliaga and M.F. Espinosa and D. Bracchitta}, url = {/brokenurl#<Go to ISI>://WOS:000347833800020}, doi = {10.4067/S0717-97072014000300020}, issn = {0717-9707}, year = {2014}, date = {2014-01-01}, journal = {Journal of the Chilean Chemical Society}, volume = {59}, number = {3}, pages = {2619-2621}, abstract = {Raman spectroscopy pigments on decorated antique Chilean pottery belonging to the Diaguita's culture deposited in Museum of Limari, have been studied by using Raman spectroscopy. Four ceramic fragments from the unknown contexts were examined. Four colors were found with certainty: red, black, brown and white. Quartz and manganese (kempite) salts, as well as different types of oxide pigments: hematite, tenorite and possibly goethite, were identified.}, keywords = {analysis, ancient, archaeology, archaeometry, art ceramics, diaguita identification, iron-oxides, pigment pigments, raman spectroscopy}, pubstate = {published}, tppubtype = {article} } Raman spectroscopy pigments on decorated antique Chilean pottery belonging to the Diaguita's culture deposited in Museum of Limari, have been studied by using Raman spectroscopy. Four ceramic fragments from the unknown contexts were examined. Four colors were found with certainty: red, black, brown and white. Quartz and manganese (kempite) salts, as well as different types of oxide pigments: hematite, tenorite and possibly goethite, were identified. |
2019 |
Methodological problems in the analysis of the Raman spectra of the paper of some postage stamps from Crete Artículo de revista Chemistry Research Journal, 4 , pp. 58-67, 2019, ISSN: 2455-8990. |
A Characterization Of Cellulose In Seven Books Using Raman Spectroscopy In The 800-1800 cm-1 Range. Artículo de revista Research Journal of Pharmaceutical, Biological and Chemical Sciences., 10 , pp. 1565-1579, 2019, ISSN: 2455-8990. |
2014 |
Micro-Raman Spectroscopy of Decorated Pottery of the Diaguita Culture from Iv Region, Chile (9th-15th Century Ad) Artículo de revista Journal of the Chilean Chemical Society, 59 (3), pp. 2619-2621, 2014, ISSN: 0717-9707. |